Q/(HG)SK 758-1998
项目Item 分析纯(AR)
含量Assay by Titration with NAOH,% ≥ 99.5-100.5
纯度Purity(HPLC) ≥99.0%
熔点范围Melting range,℃ 151.0-153.0(1,5)
醇不溶物Insoluble in alcohol,% ≤ 0.02
灼烧残渣(以硫酸盐计)Ignition residue,% ≤ 0.01
硫酸盐(SO4)Sulfate,% ≤ 0.01
重金属(以Pb计)Heavy metals,% ≤ 0.001
药用级, 99.6-101.0%
含量assay 99.6-101.0% (dry basis)
重金属heavy metals (as Pb) ≤0.001%
水分water (Karl Fischer) ≤0.2%
干燥失重loss on drying ≤0.2%
熔点Melting point 151-154 °C
阴离子anion traces
氯chloride (Cl-) ≤50 mg/kg
硝酸根nitrate (NO3-) ≤30 mg/kg
硫酸根sulfate (SO42-) ≤500 mg/kg
阳离子cation traces
砷As ≤3 mg/kg
铁Fe ≤5 mg/kg
汞Hg ≤1 mg/kg
适用性suitability passes test for appearance of solution
≥99.6%, FCC
外观Appearance White powder
红外光谱Infrared spectrum Conforms to Structure
灼烧残渣Residue on ignition (Ash) ≤0.002 %
纯度Purity (Titr. by NAOH) 99.60 - 101.00 %
熔点Melting Point 151.5 -154.0 °C
水分Water (by Karl Fischer) ≤0.20 %
砷Arsenic (As) ≤3 ppm
镉Cadmium (Cd) ≤1 ppm
汞Mercury (Hg) ≤1 ppm
铅Lead (Pb) ≤2 ppm
品级Grade 超纯级,≥99.5% (HPLC)
(Ultra pure,≥99.5% (HPLC))
外观Appearance White Powder or Crystalline Powder
红外光谱Infrared spectrometry Conforms to Structure
纯度Purity(HPLC) ≥99.5% (HPLC)
灼烧残渣ign. residue(as SO4) ≤0.05%
干燥失重loss on drying,110 °C ≤1%
氯chloride (Cl-): ≤50 ppm
硝酸盐nitrate (NO3-): ≤30 ppm
硫酸盐sulfate (SO42-): ≤500 ppm
砷As: ≤3 ppm
铜Cu: ≤10 ppm
铁Fe: ≤5 ppm
铅Pb: ≤10 ppm
锌Zn: ≤10 ppm
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