HG/T3 3-987-76
项目Item 分析纯(AR) 化学纯(CP)
含量Assay,% ≥ 99.5 99.0
熔点范围Melting range,℃ 121.0-123.0 121.0-123.0
澄清度试验Clarity 合格 合格
灼烧残渣(以硫酸盐计)Ignition residue,% ≤ 0.01 0.02
氯化合物(Cl)Chlorine compounds,% ≤ 0.01 0.03
硫化合物(以SO4计)Sulfur compounds,% ≤ 0.003 0.005
铁(Fe)Iron,% ≤ 0.0005 0.001
重金属(以Pb计)Heavy metals,% ≤ 0.001 0.001
还原高锰酸钾物质Potassium permanganate-reducing
substances 合格 --
硫酸试验Substances darkened by sulfuric acid 合格 合格
GB/T 12597-90
项目Item 基准试剂(PT)
含量(C6H5COOH)Assay,% ≥99.95-100.5% (alkalimetric)
纯度Purity(HPLC) ≥99.7%
熔点范围Melting range,℃ 121.5-123.5
澄清度试验Clarity合格
灼烧残渣(以硫酸盐计)Ignition residue,% ≤ 0.01
氯化合物(Cl)Chlorine compounds,% ≤ 0.003
硫化合物(以SO4计)Sulfur compounds ≤ 0.003
铁(Fe)Iron,% ≤ 0.0004
重金属(以Pb计)Heavy metals,% ≤ 0.0005
还原高锰酸钾物质(以O计)Potassium
permanganate-redncing substances ≤ 0.008
易炭化物质Readily carboxizable substances 合格
ACS级
项目名称Item ACS Grade
含量Assay ≥99.5%
结晶点Freezing point 122-123℃
灼烧残渣Residue after ignition ≤0.005%
甲醇不溶物Insoluble in mechanol ≤0.005%
氯化合物(Cl)Chloride compounds(as Cl) ≤0.005%
硫化物(以S计)Sulfide(S) ≤0.002%
重金属(以Pb计)Heavy metals(as Pb) ≤5ppm
还原高锰酸盐Substances reducing permanganate Passes test
≥99.5%, FCC, Kosher, FG:
外观Appearance Colorless Powder
红外光谱鉴别Infrared spectrometry Conforms to Structure
纯度Purity (Titration by NaOH) 99.5 - 100.5 %
熔点Melting point 121.0 -125.0 °C
水分Water (by Karl Fischer) ≤0.70 %
砷Arsenic (As) ≤3 ppm
镉Cadmium (Cd) ≤1 ppm
汞Mercury (Hg) ≤1 ppm
铅Lead (Pb) ≤10 ppm
杂项检测Miscellaneous Assay Pass
Passes Test (Readily Oxidizable substances And Readily Carbonizable substances)
灼烧残渣Residue on ignition (Ash) ≤0.05 %
醇溶解试验solubility in 95% Ethanol Clear Colorless ,1gm/3ml 95% Ethanol
凝固点Solidification Point 121.0 -123.0 °C
品级Grade 药典级
(Ph. Eur., BP, USP, FCC, E210)
含量assay 99.5-100.5% (alkalimetric)
可氧化物质oxidisable substances, complies
残留溶剂residual solvents, complies
重金属heavy metals (as Pb) ≤0.0005%
卤化物halogen compounds (as Cl) ≤0.03%
水分water (Karl Fischer) ≤0.7%
灼烧残渣ign. residue(as SO4) ≤0.05%
干燥损失loss on drying, 3 h (via H2SO4) ≤0.5%
pH 3-5 (20 °C, 0.1%)
熔点mp 121-125 °C
As: ≤3 ppm
Cu: ≤10 ppm
Hg: ≤1 ppm
Pb: ≤2 ppm
Zn: ≤20 ppm
溶液外观appearance of solution complies
和硫酸反应物质for reaction against H2SO4 complies
苯甲酸常以游离酸、酯或其衍生物的形式广泛存在于自然界。例如,在安息香胶内以游离酸和苄酯的形式存在,在一些植物的叶和茎皮中以游离的形式存在,在香精中以甲酯或苄酯的形式存在,在马尿中以其衍生物马尿酸的形式存在。蒸气易挥发。
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